Premium borosilicate glass 3.3 is used in XI'AN BIOLAND's precision-engineered glass distillation column thermal separation equipment. This laboratory and industrial apparatus separates up to 20 theoretical plates efficiently. Our transparent tower design and -80°C to 250°C operating temperatures enable real-time process monitoring. Our device creates vacuum below 0.1mbar with 5L to 100L capacity and configurable tower heights. This CE, ISO, UL, and SGS-certified product fulfills GMP/FDA pharmaceutical and food-grade requirements, assuring zero metallic contamination in your finished goods.
15+ Years of Manufacturing Expertise
We know your separation issues from 15 years of chemical process equipment experience. Our committed R&D team creates reliable solutions for your needs.
Complete Customization Capability
Tower diameter, height, heating techniques, pressure, and reflux ratios are customizable. We'll develop the right batch or continuous setup for your application.
Superior Material Selection
We have high-borosilicate glass, SUS304/316L stainless steel, and titanium alloy. Each substance keeps product purity in harsh chemical conditions.
Fast Delivery & Quality Assurance
We ship standard items in 5-7 days. 30 business days for custom setups. Every product is Factory Acceptance Tested before shipping.
Comprehensive Support System
Your project specialist sends weekly photographs and videos. We provide installation, commissioning, operation training, and lifetime maintenance support using genuine replacement parts.
Global Compliance
Our product systems meet GMP, FDA, CE, ISO, UL, and SGS requirements, allowing your products to access worldwide markets.
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Model |
JLF-5S |
JLF-10S |
JLF-20S |
JLF-50S |
JLF-100S |
JLF-150S |
JLF-200S |
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Distillation Tank Volume |
5L |
10L |
20L |
50L |
100L |
150L |
200L |
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Collection Tank Volume |
1L |
2L |
5L |
10L |
30L |
50L |
50L |
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Number of Collection Tanks |
1-4 sets (Customizable based on the number of fractions to be collected) |
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Stainless Steel Material |
304 Stainless Steel (Optional: 316 Stainless Steel) |
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Heating Tank |
Oil bath heater or jacket with heating liquid circulation |
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Distillation Tower Height |
Height can be customized according to the required number of theoretical plates |
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Distillation Tower Diameter |
40mm, 50mm, 80mm, 100mm or other customizable sizes |
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Distillation Tower Heating (Optional) |
Heating jacket or heating belt |
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Stirring Mode |
Magnetic stirrer, magnetic rotating stirrer or top/head stirrer (magnetic seal or mechanical seal) |
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Operating Temperature Range |
Room temperature to 300°C |
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Control System |
Digital display stirring speed controller, timer for reflux receiver/distributor, heating jacket or heating temperature controller. For oil bath heating, an additional heating temperature controller is required. |
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Accessories (Optional) |
Cooling circulator for condenser; Heater for jacketed distillation tank; Vacuum pump |
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Power Supply |
220V or 380V, 50/60HZ |
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The glass distillation column separates components efficiently using vapor-liquid equilibrium.
Vapor Generation Phase
Bottom reactors heat liquid mixtures. Lower boiling point components evaporate first, forming rising column vapour streams.
Rectification Process
Vapours ascend via precise packing materials and touch condensed liquid. Counter-current flow causes several vaporization-condensation cycles, greatly enhancing separation efficiency.
Reflux Control
Reflux from condensed overhead product returns to the column top. Automation balances product purity and throughput by controlling reflux ratio.
Product Collection
Your collecting vessel receives purified overhead product from the condenser. Heavy components stay in the bottom reactor for processing or disposal.
Visual Monitoring Advantage
Transparent glass enables you see liquid distribution, vapour patterns, and possible floods in real time, allowing process changes.
Step 1: Feed Preparation
Fill the bottom jacketed reactor with liquid. Use the control panel to set temperature and suction.
Step 2: System Stabilization
Turn on vacuum and heater. The system stabilizes around 30-60 minutes, depending on capacity.
Step 3: Distillation Operation
Track the column temperature gradient. Optimize separation with reflux ratio and heating power. PID controls exact temperature zones.
Step 4: Product Collection
Collect purified fractions at temperature cuts. Transparency helps detect component transition zones.
Step 5: Continuous Monitoring
Track column pressure decrease, reflux, and liquid levels during operation. We support batch and continuous feeding.
Step 6: Shutdown & Cleaning
The smooth glass surface simplifies CIP (Clean-in-Place) after each run, prepping the system rapidly for your next batch.
Pharmaceutical Manufacturing
DCM, ethyl acetate, and acetone from API synthesis may be recovered and purified. For pharmaceutical intermediates, the inert glass surface avoids metallic contamination and meets GMP standards.
Essential Oil Processing
Vacuum fractional distill heat-sensitive floral extracts. Reduce unstable terpenes and concentrate oxygenated chemicals to retain sensitive aromatic characteristics.
Chemical Synthesis
Make excellent chemicals by purifying reaction products. This corrosion-resistant design can withstand acids, chlorinated solvents, and other harsh environments that erode metal equipment.
Petrochemical Research
Analyze crude oil and fuel composition. Researchers use optical transparency to study hydrocarbon separation patterns and adjust refinery settings.
Food & Beverage Industry
Recover food-grade ethanol from flavourings. Ingredients that fulfill FDA criteria assure product safety.
Cosmetics Production
Purify scent and natural substances. The clean atmosphere retains high skincare and perfume quality.
To guarantee every unit meets worldwide standards, XI'AN BIOLAND has complete quality management systems:
Material inspection, welding verification, pressure testing, and thorough functional testing precede shipping for quality control.
Q: What's the difference between glass and stainless steel distillation columns?
A: Glass columns provide complete visual process monitoring and prevent metallic contamination. They're ideal for corrosive chemicals and pharmaceutical applications. Stainless steel offers higher pressure ratings and durability for large-scale industrial production.
Q: How do I select the appropriate column capacity?
A: Take into account batch size, processing time, and space. Our technical staff will determine the best capacity for your feed mix and separation needs. Contact info@biolandequip.com for customized advice.
Q: Can you operate products under vacuum?
A: Our systems reach vacuum sub 0.1mbar. Vacuum operation decreases boiling points, safeguarding heat-sensitive materials and enhancing high-boiling compound separation.
Q: What packing material should I choose?
A: Glass Raschig rings are chemically resistant for corrosive applications. Stainless steel θ rings offer increased capacity and less pressure drop. Small laboratory columns benefit from glass springs. Based on your procedure, we'll provide the optimal choice.
Q: What's included in your customization service?
A: We customize tower dimensions, heating methods, control systems, material selection, pressure ratings, and reflux configurations. Share your process requirements, and we'll design a complete solution with detailed engineering drawings for your approval.
Q: How long does delivery take?
A: Standard configurations ship within 5-7 business days. Customized systems typically deliver in 30 business days. We'll provide weekly progress updates with photos throughout manufacturing.
Q: What after-sales support do you provide?
A: We offer a one-year warranty with lifetime maintenance support. Our services include installation guidance, operation training, troubleshooting assistance, and stocked spare parts. Technical support is available whenever you need it.
Q: Can the system handle corrosive acids?
A: Absolutely. Borosilicate glass 3.3 provides Class 1 acid resistance, withstanding concentrated sulfuric acid, nitric acid, and hydrochloric acid. This makes our columns ideal for acid recovery and concentration applications.
Ready to upgrade your separation process with glass distillation column? Reach out to our technical team at info@biolandequip.com for customized solutions and quotations today.
2024-05-16
Pharmaceutical Company
The reactor is beautifully mirror-polished and fully complies with GMP requirements for the pharmaceutical industry. The performance is excellent! Overall, we are very satisfied! We also provided with some feedback on our process improvements, which we hope will be helpful.
2024-04-09
Laboratory
Excellent and professional service. Always reply our questions very fast. All reactors and chiller we received are good too.
2024-02-15
Research Institute
Quality is beyond our expectation actually. After we got the extraction equipment and started using it, the performance was beyond our expectation. Very easy to use and very efficient to run. Service always respond us very quickly. Was also very helpful to help us. Thanks Bioland team. Very happy to work with you.
2023-11-20
Biotech Company
We are happy about the new purchase as always. Equipment and services are both good.
2023-08-05
Instrument Lab
This is the second order with Bioland instrument and everything is good as the first dateText.
2023-05-12
Global Trading Partner
Bioland instrument team is very helpful and professional. The sales helped us select the right equipment for our application, and their logistics people handled the transportation and customs declaration for our shipment. All that saved us a lot of work.
